Simple Setup Miniaturization with Multiple Benefits for Green Chemistry in Nanoparticle Synthesis
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The development of nanomaterials often relies on wet-chemical synthesis performed in reflux setups using round-bottom flasks. Here, an alternative approach to synthesize nanomaterials is presented that uses glass tubes designed for NMR analysis as reactors. This approach uses less solvent and energy, generates less waste, provides safer conditions, is less prone to contamination, and is compatible with high-throughput screening. The benefits of this approach are illustrated by an in breadth study with the synthesis of gold, iridium, osmium, and copper sulfide nanoparticles.
| Original language | English |
|---|---|
| Journal | ACS Omega |
| Volume | 7 |
| Issue number | 5 |
| Pages (from-to) | 4714-4721 |
| Number of pages | 8 |
| ISSN | 2470-1343 |
| DOIs | |
| Publication status | Published - 2022 |
Bibliographical note
Funding Information:
This project has received funding from the European Union’s Horizon 2020 research and innovation program under the Marie Sklodowska-Curie grant agreement No. 840523 (CoSolCat, JQ) and 841903 (SRC). This project has received funding from the Villum Foundation through a Villum Young Investigator grant (VKR00015416) and the Danish National Research Foundation (DNRF 149) Center for High-Entropy Alloy Catalysis (CHEAC). This research used resources of the Advanced Photon Source, a U.S. Department of Energy (DOE) Office of Science User Facility, operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357 (GUP-73929).
Publisher Copyright:
© 2022 The Authors. Published by American Chemical Society.
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